Implementation Protocols
Comprehensive field protocols refined through nearly 2,000 successful projects, featuring proprietary injection systems and automated monitoring technology
ISCO Implementation
Step-by-step protocols for in-situ chemical oxidation projects from design through completion
Implementation Phases
Phase 1
Pre-Implementation Planning
- 1.Review site characterization data and conceptual site model
- 2.Conduct bench-scale treatability testing if needed
- 3.Calculate reagent demand using soil/groundwater data
- 4.Design injection grid spacing (typically 10-20 ft radius of influence)
- 5.Prepare Health & Safety Plan and Site-Specific Work Plan
- 6.Obtain necessary permits and regulatory approvals
- 7.Coordinate site access and utility clearances
- 8.Schedule pre-injection groundwater sampling
Phase 2
Field Mobilization
- 1.Mobilize direct push rig or drilling equipment
- 2.Stage reagents and mixing equipment
- 3.Establish exclusion zones and safety protocols
- 4.Conduct pre-injection site meeting
- 5.Install temporary monitoring points if needed
- 6.Set up real-time monitoring equipment
- 7.Verify injection point locations via utility clearance
Phase 3
Injection Execution
- 1.Mix reagents to specified concentrations (e.g., 40% NaMnO4, 15% persulfate)
- 2.Use direct push equipment (Geoprobe 7720DT, AMS 9600/9700 series)
- 3.Advance probe to target depth intervals (typically 2-5 ft intervals)
- 4.Inject reagent solution at controlled pressure/flow rate (<150 psi)
- 5.Monitor injection pressure and refusal conditions
- 6.Document injection volumes and depths per location
- 7.Use expendable, retractable, or sealed pressure-activated injection points
- 8.Collect soil cores for visual confirmation of reagent distribution
- 9.Measure oxidant residuals in observation wells
- 10.Real-time flow monitoring with pulsation dampeners for accurate measurement
- 11.Adjust injection parameters based on field observations
Phase 4
Post-Treatment Monitoring
- 1.Collect post-injection groundwater samples (2-4 weeks)
- 2.Analyze for target contaminants and geochemical parameters
- 3.Monitor oxidant residuals and pH
- 4.Evaluate treatment effectiveness vs. cleanup goals
- 5.Conduct quarterly monitoring for 12-24 months
- 6.Perform additional injections if needed
- 7.Prepare completion report and closure documentation
Key Implementation Parameters
- •Reagent type and concentration (e.g., 40% NaMnO4, 10-20% persulfate)
- •Injection spacing: 10-20 ft radius of influence
- •Soil oxidant demand (SOD): typically 5-7.5 g/kg for NOM
- •Natural Organic Matter (NOM) demand via TCLP testing
- •pH adjustment requirements for persulfate activation
- •Injection pressure limits: <150 psi for most formations
- •Target oxidant residuals: maintain first-order kinetics
- •Swag factor: typically 2x calculated demand for field conditions
Health & Safety Requirements
- ⚠PPE: Tyvek suits, chemical gloves, safety glasses, respirators if needed
- ⚠Heat stress monitoring for activated persulfate
- ⚠Vapor monitoring during injection
- ⚠Emergency response procedures for spills
- ⚠Decontamination procedures
Quality Control & Assurance
Pre-Treatment QC
Verify site characterization data accuracy
Confirm reagent specifications and quality
Calibrate injection equipment
Conduct pre-treatment site inspection
Review and approve health & safety plan
During Treatment QC
Real-time monitoring of injection parameters
Field measurements (pH, ORP, temperature)
Visual observations and photo documentation
Daily progress reports
Equipment performance checks
Post-Treatment QC
Collect representative verification samples
Third-party laboratory analysis
Data validation and quality review
Compare results to cleanup goals
Statistical analysis of treatment effectiveness
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